HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Carbonate → HCID 178509280, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Edukt | N-(2-((4-chlorophenethyl)(piperidin-4-yl)amino)ethyl)benzamide | HCID 121410331 | — |
| Edukt | HCID 131737066 | HCID 131737066 | — |
| Produkt | HCID 178509280 | HCID 178509280 | — |
Reaktionsschritte
N-(2-((4-Chlorophenethyl)(piperidin-4-yl)amino)ethyl)benzamide obtained in Step 4 was reacted with K2CO3 and S,S′-dimethyl-N-cyano-dithioiminocarbonate, followed by the cyclization of the intermediate (N-cyanopiperazine-1-carbimidothioate) with hydrazine monohydrate in a manner described in Procedure 3. Purification over silica gel provided pure product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09440953B2 |
| Quelldatensatz | uspto-grants-2016_09 |
| ORD ID | ord-74267245d16542a2bcfaf4369e448bf8 |
| Quellennotiz | uspto-grants-2016_09 |