Diethyl (ethoxymethylene)malonate → HCID 2268087, compound

Participants

Reaction Conditions

Reaction Steps

3-Bromoaniline (10.0 g, 47 mmol) was dissolved in abs. ethanol (100 mL). Diethyl ethoxymethylenemalonate (10.2 g, 47 mmol) was added. The solution stirred at 80° C. overnight. The solution was slowly cooled and a precipitant formed. The product was filtered and dried to give 12.6 g (70%) of the title compound.

Provenance & Evidence