HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58938674, compound → HCID 58938656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58938674 | HCID 58938674 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Palladium | HCID 23938 | — |
| Product | HCID 58938656 | HCID 58938656 | 100.3% |
Reaction Steps
1-(Dipropylamino)-6-mesityl-3-vinyl-4H-quinolizine-4-one (9.4 mg, 0.024 mmol) was dissolved in methanol (1 mL) 10 mg of 10% Pd/C was added. The solution was evacuated and filled with a hydrogen balloon at room temperature. After 1 h, the solution was filtered and concentrated. Flash chromatography (5% ethyl acetate/hexanes) gave 9.4 mg (100% yield) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897607B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-0f88a640c3f54a2fa69c6272a2c2f08e |
| Source note | uspto-grants-2011_03 |