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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 598180Generated: October 30, 2026

N-bromobutanimide → HCID 58938574, compound

https://huagongshe.com/reaction/598180

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-bromobutanimideHCID 67184—
ReactantHCID 58938600HCID 58938600—
SolventDimethylformamideHCID 6228—
ProductHCID 58938574HCID 5893857490%

Reaction Conditions

Temperature0 °C

Reaction Steps

1-Benzyl-5-mesitylquinolin-4(1H)-one (0.52 g, 1.5 mmol) was dissolved in N,N-dimethylformamide (10 mL) and cooled to 0° C. N-bromosuccinimide (0.27 g, 1.5 mmol) was added and the reaction stirred for 1 hr. The reaction was quenched with water (100 mL) and the precipitate was collected by vacuum filtration. 0.57 g (90%) of the title compound was obtained as a yellow solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07897607B2
Source datasetuspto-grants-2011_03
ORD IDord-b66ae0bd0e994bcba1a5f6ebf975e3aa
Source noteuspto-grants-2011_03