HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 598180Generated: October 30, 2026
N-bromobutanimide → HCID 58938574, compound
https://huagongshe.com/reaction/598180
Participants
| Role | Name | HCID | Charge |
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| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 58938600 | HCID 58938600 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 58938574 | HCID 58938574 | 90% |
Reaction Steps
1-Benzyl-5-mesitylquinolin-4(1H)-one (0.52 g, 1.5 mmol) was dissolved in N,N-dimethylformamide (10 mL) and cooled to 0° C. N-bromosuccinimide (0.27 g, 1.5 mmol) was added and the reaction stirred for 1 hr. The reaction was quenched with water (100 mL) and the precipitate was collected by vacuum filtration. 0.57 g (90%) of the title compound was obtained as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07897607B2 |
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| Source dataset | uspto-grants-2011_03 |
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| ORD ID | ord-b66ae0bd0e994bcba1a5f6ebf975e3aa |
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| Source note | uspto-grants-2011_03 |
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