Hexyl isocyanate → HCID 86628808, compound

HRID 598203Notes

Reaction equation

HRID 598203 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][N:5]=[C:4]2[NH:8][C:9](=[O:18])[N:10]([C:11]([O:13][C:14]([CH3:17])([CH3:16])[CH3:15])=[O:12])[C:3]=12.[N:19]([CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27])=[C:20]=[O:21]>O1CCOCC1>[CH2:22]([NH:19][C:20]([N:8]1[C:4]2=[N:5][CH:6]=[CH:7][C:2]([CH3:1])=[C:3]2[N:10]([C:11]([O:13][C:14]([CH3:15])([CH3:17])[CH3:16])=[O:12])[C:9]1=[O:18])=[O:21])[CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]

Participants

4

Reactant 2

HCID 75659Hexyl isocyanateHCID 67268948HCID 67268948, compound

Product 1

HCID 86628808HCID 86628808, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

Analogously to Example 1, tert-butyl 7-methyl-2-oxo-2,3-dihydroimidazo[4,5-b]pyridine-1-carboxylate (200 mg, 0.8 mmol) and 1-isocyanatohexane (113 mg, 0.88 mmol) were reacted in dioxane. Yield: 5 mg (2%), M+H+: 377.20.

Sources & evidence

ORD record
ord-17a39afaf907484497d40187e80dbaaf
Source dataset
uspto-grants-2011_03
Patent number
US07897616B2

Reaction notes

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