HuagongsheHuagongshe Chemistry Print Report · For research reference only
(7-Benzyloxy-3-nitroquinolin-4-yl)-(2-phenoxyethyl)amine → 6-(benzyloxy)-N4-methylquinoline-3,4-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (7-Benzyloxy-3-nitroquinolin-4-yl)-(2-phenoxyethyl)amine | HCID 67050949 | — |
| Reactant | N-(6-benzyloxy-5-nitroquinolin-4-yl)-N-methylamine | HCID 67051134 | — |
| Product | 6-(benzyloxy)-N4-methylquinoline-3,4-diamine | HCID 67051007 | — |
Reaction Steps
The general method described in Part B of Example 46 was followed using N-(6-benzyloxy-5-nitroquinolin-4-yl)-N-methylamine (11.36 g, 36.7 mmol) in lieu of (7-benzyloxy-3-nitroquinolin-4-yl)-(2-phenoxyethyl)amine. 6-Benzyloxy-N4-methylquinoline-3,4-diamine (7.91 g) was obtained as a dark yellow oil and used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897597B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-c9f1404348794c79954c2f03b5bd48e7 |
| Source note | uspto-grants-2011_03 |