HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzeneacetonitrile, 4-fluoro- → HCID 73053293, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzeneacetonitrile, 4-fluoro- | HCID 68016 | — |
| Reactant | 1-(4-chloro-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole | HCID 90032549 | — |
| Product | HCID 73053293 | HCID 73053293 | — |
Reaction Steps
The title compound, yellow solid (28 mg, 22%), MS (ISP) m/z=390.2 [(M+H)+], mp 154° C., was prepared in accordance with the general method of example 1 from 1-(4-chloro-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole (intermediate H) (100 mg, 353 μmol) and commercially available 2-(4-fluoro-phenyl)-acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440962B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-6e2a579562844b8e857c1de655931736 |
| Source note | uspto-grants-2016_09 |