HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetonitrile → 3-Phenyl-5-(2-phenyl-2H-pyrazol-3-yl)-benzo[c]isoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetonitrile | HCID 8794 | — |
| Reactant | 5-(4-Nitrophenyl)-1-phenyl-1H-pyrazole | HCID 13287219 | — |
| Product | 3-Phenyl-5-(2-phenyl-2H-pyrazol-3-yl)-benzo[c]isoxazole | HCID 73050960 | — |
Reaction Steps
The title compound, light grey solid (37 mg, 29%), MS (ISP) m/z=338.3 [(M+H)+], mp 163° C., was prepared in accordance with the general method of example 1 from 5-(4-nitro-phenyl)-1-phenyl-1H-pyrazole (intermediate A) (100 mg, 353 μmol) and commercially available 2-phenyl-acetonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440962B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-6205c395f8cb41608996a9d2a6bc054c |
| Source note | uspto-grants-2016_09 |