Ammonia → HCID 67152148, compound

Participants

Reaction Steps

Prepared from (4r)-1-azatricyclo[3.3.1.13,7]dec-4-ylamine hydrochloride and benzothiazole-6-carboxylic acid (Maybridge); yield 129 mg, 0.33 mmol (91%) according to methods A and C: 1H NMR (300 MHz, methanol-d4) δ 2.10-2.30 (m, 6H), 2.50 (s, 2H), 3.51 (d, J=12 Hz, 2H), 3.57 (s, 2H), 3.87 (d, J=13 Hz, 2H), 4.31 (s, 1H), 8.08 (dd, J=9, 2 Hz, 1H), 8.16 (d, J=9 Hz, 1H), 8.69 (d, J=2 Hz, 1H), 9.49 (s, 1H); MS (DCI/NH3) m/z 314 (M+H)+; Anal. C17H19N3OS.2HCl.0.4H2O: C, H, N.

Provenance & Evidence