Ammonia → HCID 16067940, compound

Participants

Reaction Steps

Prepared from (4s)-1-azatricyclo[3.3.1.13,7]dec-4-ylamine and 3-chlorobenzoic acid (Aldrich) according to method B; 1H NMR (500 MHz, methanol-d4) δ 1.84-2.05 (m, 5H), 2.11 (s, 1H), 2.29 (s, 1H), 2.32 (s, 1H), 2.39 (s, 2H), 3.47-3.53 (m, 2H), 3.62-3.74 (m, 1H), 3.77-3.88 (m, 1H), 4.38 (s, 1H), 7.43-7.52 (m, 1H), 7.54-7.61 (m, 1H), 7.73-7.80 (m, 1H), 7.78-7.88 (m, 1H); MS (APCI/NH3) m/z 291 (M+H)+.

Provenance & Evidence