HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 67152131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3-Fluorobenzoic Acid | HCID 9968 | — |
| Reactant | 1-Azatricyclo[3.3.1.1,3,7]decan-4-amine | HCID 15686618 | — |
| Product | HCID 67152131 | HCID 67152131 | — |
Reaction Steps
Prepared from (4s)-1-azatricyclo[3.3.1.13,7]dec-4-ylamine and 3-fluorobenzoic acid (Aldrich) according to method B; 1H NMR (500 MHz, methanol-d4) δ 1.88-1.98 (m, 3H), 2.03 (s, 1H), 2.26-2.33 (m, 4H), 3.42 (s, 2H), 3.48-3.56 (m, 4H), 4.37 (s, 1H), 7.27-7.32 (m, 1H), 7.44-7.53 (m, 1H), 7.55-7.62 (m, 1H), 7.66 (d, J=8 Hz, 1H); MS (APCI/NH3) m/z 275 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897766B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-ac9c48d30295429e8863df91203fc020 |
| Source note | uspto-grants-2011_03 |