HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 16068163, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 2-Naphthoic acid | HCID 7123 | — |
| Reactant | 1-Azatricyclo[3.3.1.1,3,7]decan-4-amine | HCID 15686618 | — |
| Product | HCID 16068163 | HCID 16068163 | — |
Reaction Steps
Prepared from (4s)-1-azatricyclo[3.3.1.13,7]dec-4-ylamine and 2-naphthoic acid (Aldrich) according to method B; 1H NMR (500 MHz, methanol-d4) δ 1.94-2.03 (m, 3H), 2.29-2.40 (m, 4H), 3.40 (s, 2H), 3.51 (s, 4H), 4.43 (s, 1H), 7.54-7.62 (m, 2H), 7.86-8.02 (m, 4H), 8.40 (d, J=1 Hz, 1H); MS (APCI/NH3) m/z 307 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897766B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-48901d962973468cbbf325a307cc948a |
| Source note | uspto-grants-2011_03 |