HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanesulfinate → HCID 118235388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanesulfinate | HCID 2733271 | — |
| Reactant | 2-Bromo-4-ethyl-5-nitropyridine | HCID 40151872 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 118235388 | HCID 118235388 | — |
Reaction Steps
A mixture of 2-bromo-4-ethyl-5-nitro-pyridine (4.35 mmol) and sodium methanesulfinate (4.35 mmol) in DMSO (10 mL) was stirred at room temperature for 1.5 h. The mixture was poured into ice-water and stirred until the ice had melted. The mixture was filtered and the solid (the desired product) was collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09440929B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-78c5fd9b5c2b42559f40683b7d871ded |
| Source note | uspto-grants-2016_09 |