Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Trifluoromethyl)benzylamine → 4-((4-(Trifluoromethyl)benzyl)amino)benzo[d][1,2,3]triazine-8-carboxamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Trifluoromethyl)benzylamine | HCID 76804 | — |
| 반응물 | 4-oxo-1H-1,2,3-benzotriazine-8-carboxamide | HCID 178513613 | — |
| 생성물 | 4-((4-(Trifluoromethyl)benzyl)amino)benzo[d][1,2,3]triazine-8-carboxamide | HCID 76073579 | — |
반응 단계
Compound 8 was prepared following general synthetic scheme 7 wherein (4-(trifluoromethyl)phenyl)methanamine was reacted with 4-hydroxybenzo[d][1,2,3]-triazine-8-carboxamide to give the title compound. LC-MS [348 (M+1)], 1H NMR (400 MHz, DMSO-d): δ 9.40-9.37 (m, 2H), 8.56-8.51 (m, 2H), 8.05 (s, 1H), 8.01 (t, 1H), 7.70 (d, 2H), 7.62 (d, 2H), 4.99 (d, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09440968B2 |
| 출처 데이터셋 | uspto-grants-2016_09 |
| ORD ID | ord-49c2dd3240b64c2f8544b65165772e71 |
| 출처 메모 | uspto-grants-2016_09 |