HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Cresol → HCID 57835403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | HCID 67272809 | HCID 67272809 | — |
| Solvent | Boron trifluoride etherate | HCID 8000 | — |
| Product | HCID 57835403 | HCID 57835403 | 78% |
Reaction Steps
5-(1-Ethyl-propenyl)-benzo[b]thiophene-2-carboxylic acid ethyl ester (5.50 g, 20.0 mmol), o-cresol (4.33 g, 40.0 mmol), and BF3-Et2O (10 mL) are reacted analogous to Example 1C to afford the title compound (5.97 g, 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897789B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-5fadbb9db0a8464ab54da15e2ecd20ab |
| Source note | uspto-grants-2011_03 |