HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 57835413, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 57835421 | HCID 57835421 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57835413 | HCID 57835413 | 86.3% |
Reaction Steps
2-{1-[4-(3,3-Dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethyl-propyl}-benzo[b]thiophene-6-carboxylic acid methyl ester (4.50 g, 9.64 mmol) in THF (100 mL) is reacted with NaBH4 (0.37 g, 9.64 mmol) analogous to Example 2 to obtain the title compound (3.90 g, 86%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07897789B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-dd6810004803450d9960f06dc4c20559 |
| Source note | uspto-grants-2011_03 |