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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 6001Generated: October 26, 2026

3-Cyanophenol → O-3-cyanophenyl dimethylthiocarbamate

https://huagongshe.com/reaction/6001

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-CyanophenolHCID 13394—
ReactantPotassium HydroxideHCID 14797—
ReactantDimethylthiocarbamoyl chlorideHCID 27871—
ProductO-3-cyanophenyl dimethylthiocarbamateHCID 14795402—

Reaction Steps

If the procedure described in Preparation XI is followed starting from 15 g (126.10-3 mol) of 3-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (132.10-3 mol) of potassium hydroxide, 29 g (quantitative yield) of the expected product are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05246961
Source datasetuspto-grants-1993_09
ORD IDord-b26089eaf91d4f27b4272b0ec41c29a8
Source noteuspto-grants-1993_09