HCID 58836075, compound → HCID 67057403, compound

HRID 600158Notes

Reaction equation

HRID 600158 reaction equation
[C:1]1([CH3:31])[CH:6]=[CH:5][C:4]([NH:7][C:8]2[C:13]([NH:14][C:15]3[CH:20]=[CH:19][C:18]([CH3:21])=[CH:17][CH:16]=3)=[CH:12][CH:11]=[CH:10][C:9]=2[C:22]2[S:26][C:25]3[CH:27]=[CH:28][CH:29]=[CH:30][C:24]=3[CH:23]=2)=[CH:3][CH:2]=1.[Br:32]C1C=CC2C(C3C=CC(C)=CC=3)=C(C3C=CC(C)=CC=3)SC=2C=1>>[Br:32][C:10]1[C:9]([C:22]2[S:26][C:25]3[CH:27]=[CH:28][CH:29]=[CH:30][C:24]=3[CH:23]=2)=[C:8]([NH:7][C:4]2[CH:3]=[CH:2][C:1]([CH3:31])=[CH:6][CH:5]=2)[C:13]([NH:14][C:15]2[CH:20]=[CH:19][C:18]([CH3:21])=[CH:17][CH:16]=2)=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 58836075HCID 58836075, compoundHCID 67057479HCID 67057479, compound

Product 1

HCID 67057403HCID 67057403, compound

Procedure

Intermediate C was synthesized in the same manner as in Synthesis Example 1, except that 2,3-di-p-tolylaminophenyl-benzo[b]thiophene was used instead of 2,3-di-p-tolyl-benzo[b]thiophene used to synthesize Intermediate B in Synthesis Example 1.

Workup

  1. customin Synthesis Example 1

Sources & evidence

ORD record
ord-78519a7af41f4b539a14882dcf63970b
Source dataset
uspto-grants-2011_03
Patent number
US07901793B2

Reaction notes

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