HRID6002

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11591

Mercuric cyanide

C2HgN2

结构：CC(=O)O[C@@H]1[C@@H](OC(C)=O)[C@@H](Br)SC[C@H]1OC(C)=O

HCID10926314

未命名化合物

HCID14795334

3-Sulfanylbenzonitrile

C7H5NS

PRODUCTS

生成物

结构：CC(=O)O[C@@H]1[C@@H](OC(C)=O)[C@H](Sc2cccc(C#N)c2)SC[C@H]1OC(C)=O

HCID14795343

未命名化合物

PROCEDURE

实验过程

If the procedure described in Preparation I is followed starting from 9.3 g (67.10-3 mol) of 3-mercaptobenzonitrile, 18 g (73.10-3 mol) of mercuric cyanide, Hg(CN)2, and 26.14 g (73.10-3 mol) of 2,3,4-tri-O-acetyl-5-thio-α-D-xylopyranosyl bromide, 8.55 g of the expected product are obtained.

WORKUP

后处理

customIf the procedure described in Preparation I