Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 6004Generated: October 25, 2026

2-Hydroxybenzonitrile → O-2-cyanophenyl dimethylthiocarbamate

https://huagongshe.com/reaction/6004

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-HydroxybenzonitrileHCID 11907—
ReactantPotassium HydroxideHCID 14797—
ReactantDimethylthiocarbamoyl chlorideHCID 27871—
ProductO-2-cyanophenyl dimethylthiocarbamateHCID 1479540394%

Reaction Steps

If the procedure described in Preparation XVI is followed starting from 15 g (126.10-3 mol) of 2-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (126.10-3 mol) of potassium hydroxide, 24.1 g (yield: 94%) of the expected product are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05246961
Source datasetuspto-grants-1993_09
ORD IDord-0e3bf4991a3f466d9c41ae0105fc4554
Source noteuspto-grants-1993_09