HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53416493, compound → HCID 67228763, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53416493 | HCID 53416493 | — |
| Reactant | 2-Ethoxy-8-isothiocyanato-1,4-dihydronaphthalene | HCID 86609612 | — |
| Reactant | HCID 86609614 | HCID 86609614 | — |
| Reactant | HCID 86609615 | HCID 86609615 | — |
| Product | HCID 67228763 | HCID 67228763 | 16% |
Reaction Steps
The title compound was prepared using the procedure as described in Example 1H, substituting the product of Example 20F (415 mg, 1.36 mmol) for the product of Example 1F and the product of Example 22A (404 mg, 1.63 mmol) for the product of Example 1G. The crude product was purified by flash chromatography eluting with 20% to 60% EtOAc/hexanes which gave 107 mg (16%) of the title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902236B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-8a3701485d6247e7843411af5deb8e45 |
| Source note | uspto-grants-2011_03 |