HRID600847

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID75140

p-(Dimethoxymethyl)anisole

C10H14O3

结构：CC(C)(C)OC(=O)N1C(C)(C)OC[C@@]1(CNc1cccc(Cl)c1)C(C)(C)C

HCID67271544

未命名化合物

PRODUCTS

生成物

结构：COc1ccc(CN(C[C@H]2COC(C)(C)N2C(=O)OC(C)(C)C)c2cccc(Cl)c2)cc1

HCID57667078

未命名化合物

PROCEDURE

实验过程

In analogy to example 20.a tert-butyl (S)-4-[(3-chloro-phenylamino)-methyl]-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester was reacted with p-anisaldehyde dimethyl acetal to give (S)-4-{[(3-chloro-phenyl)-(4-methoxy-benzyl)-amino]-methyl}-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester. White solid. MS (ISP): 463.1 ([{37Cl}M+H]+), 461.1 ([{35Cl}M+H]+)