HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 619795, compound → HCID 58976855, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 619795 | HCID 619795 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 58976855 | HCID 58976855 | — |
Reaction Steps
The crude acetamide was dissolved in EtOAc (50 mL), shacked with 10% Pd/C (450 mg) under H2 (50 psi) for 3 h. Filtration gave an N-(5-amino-2-fluoro-phenyl)-2,2,2-trifluoro-acetamide (8.42 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902239B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-db933a25babf4a8a9d777eb43e49b022 |
| Source note | uspto-grants-2011_03 |