HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentafluoroaniline → 501670-16-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentafluoroaniline | HCID 13040 | — |
| Reactant | 3,5-Di-tert-butylsalicylaldehyde | HCID 688023 | — |
| Reactant | 2,4-Bis(tert-butyl)-6-[[(2,6-dibromophenyl)imino]methyl]phenol | HCID 136346710 | — |
| Product | 501670-16-2 | HCID 135509894 | — |
Reaction Steps
Employing an analogous procedure to that described above for the synthesis of 2,4-bis(tert-butyl)-6-[[(2,6-dibromophenyl)imino]methyl]phenol, 2,3,4,5,6-pentafluoroaniline (0.54 g, 2.9 mmol) was added to 3,5-di-tert-butyl-2-hydroxybenzaldehyde (0.70 g, 2.9 mmol). The product was purified by recrystallisation from hot MeOH and isolated as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902308B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-1224c7f7869c44258aeb252783b2e5e7 |
| Source note | uspto-grants-2011_03 |