Sodium borohydride → HCID 86761287, compound

Participants

Role	Name	HCID	Charge
Reactant	Sodium borohydride	HCID 4311764	—
Reactant	2,4-Bis(tert-butyl)-6-[[(2,6-dibromophenyl)amino]methyl]phenol	HCID 86627667	—
Reactant	2,4-Di-tert-butyl-6-[(pentafluoroanilino)methylidene]cyclohexa-2,4-dien-1-one	HCID 135509894	—
Product	HCID 86761287	HCID 86761287	—

Reaction Steps

Using an analogous procedure to the synthesis of 2,4-bis(tert-butyl)-6-[[(2,6-dibromophenyl)amino]methyl]phenol described above, NaBH4 (1.2 g) was added to a solution of 2,4-bis(tert-butyl)-6-[[(2,3,4,5,6-pentafluorophenyl)imino]methyl]phenol (0.5 g, 1.25 mmol). The product was isolated as an air sensitive white solid, and stored under nitrogen. Yield 0.48 g, 95%.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07902308B2
Source dataset	uspto-grants-2011_03
ORD ID	ord-cf383229a0df4fa59e8081ce6158a8fb
Source note	uspto-grants-2011_03