Ethyl 2-{[2-(1-cyclohexen-1-yl)ethyl]amino}nicotinate → 1-[2-(1-cyclohexen-1-yl)ethyl]-2H-pyrido[2,3-d][1,3]oxazine-2,4(1H)-dione

HRID 601111Notes

Reaction equation

HRID 601111 reaction equation
[C:1]1([CH2:7][CH2:8][NH:9][C:10]2[N:20]=[CH:19][CH:18]=[CH:17][C:11]=2[C:12]([O:14][CH2:15]C)=[O:13])[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1.C(C(CC)CNC1N=CC=CC=1C(OCC)=[O:29])C>>[C:1]1([CH2:7][CH2:8][N:9]2[C:10]3[N:20]=[CH:19][CH:18]=[CH:17][C:11]=3[C:12](=[O:13])[O:14][C:15]2=[O:29])[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1

Participants

3

Reactant 2

HCID 63539637Ethyl 2-{[2-(1-cyclohexen-1-yl)ethyl]amino}nicotinateHCID 67064133Ethyl 2-[(2-ethylbutyl)amino]nicotinate

Product 1

HCID 865921051-[2-(1-cyclohexen-1-yl)ethyl]-2H-pyrido[2,3-d][1,3]oxazine-2,4(1H)-dione

Procedure

The title compound was prepared according to the procedure of Example 3B substituting the product of Example 45A for the product of Example 3A (0.493 g, 91%). MS (DCI) m/z 290 (M+NH4)+.

Sources & evidence

ORD record
ord-f77b7fada0c44971af81623064dabd66
Source dataset
uspto-grants-2011_03
Patent number
US07902203B2

Reaction notes

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