Ammonia → HCID 86592120, compound

HRID 601151Notes

Reaction equation

[CH2:1]([NH:8][C:9]1[N:10]=[C:11]([S:18][CH3:19])[S:12][C:13]=1[C:14]([O:16][CH3:17])=[O:15])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(C(CC)CNC1N=CC=CC=1C(OCC)=[O:28])C.N>>[CH2:1]([N:8]1[C:9]2[N:10]=[C:11]([S:18][CH3:19])[S:12][C:13]=2[C:14](=[O:15])[O:16][C:17]1=[O:28])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

Reactant 3

HCID 222Ammonia

HCID 67063638HCID 67063638, compound

HCID 67064133Ethyl 2-[(2-ethylbutyl)amino]nicotinate

Product 1

HCID 86592120HCID 86592120, compound

Procedure

The title compound was prepared according to the procedure of Example 3B substituting the product of Example 139A for the product of Example 3A (0.048 g, 92%). MS (DCI/NH3) m/z 324 (M+NH4)+.

Sources & evidence

ORD record: ord-5c5061ca23c6427cb72b25bfaaa113b1
Source dataset: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07902203B2

Reaction notes

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