HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → (E)-2-(2-Benzylidenehydrazinyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Benzoic acid, 2-hydrazinyl-, hydrochloride (1:1) | HCID 104169 | — |
| Product | (E)-2-(2-Benzylidenehydrazinyl)benzoic acid | HCID 9561044 | — |
Reaction Steps
The title compound was prepared from 2-hydrazinobenzoic acid hydrochloride (1.89 g, 10.0 mmol) and benzaldehyde (1.06 g, 10.0 mmol) according to the procedure of Fischer, E. and co-workers described in Chem. Ber., 35, 1902, 2318 (2.4 g, quantitative yield). MS (DCI) m/z 241 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902203B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-6d1024f6a29240f0b05f02af51dcb53d |
| Source note | uspto-grants-2011_03 |