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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 60126Generated: October 29, 2026

1,4-Dioxane hydrochloride → HCID 117776661, compound

https://huagongshe.com/reaction/60126

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,4-Dioxane hydrochlorideHCID 20443148—
ReactantTert-butyl (2-(3-fluorophenyl)-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-7-yl)carbamateHCID 90383257—
ProductHCID 117776661HCID 117776661—

Reaction Steps

A 4 N hydrochloric acid-1,4-dioxane solution (5 ml) was added to the tert-butyl (2-(3-fluorophenyl)-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-7-yl)carbamate (116 mg) obtained in (Example 2.7) <Step 5>, and the obtained mixture was then stirred for 1 hour. Thereafter, the solvent was distilled away under reduced pressure, and the title compound (133 mg) was obtained in the form of a colorless solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09440970B2
Source datasetuspto-grants-2016_09
ORD IDord-3c29896fc1944183aea0bb3bc83741e1
Source noteuspto-grants-2016_09