HCID 21331325, compound → HCID 23158201, compound

HRID 601659Notes

Reaction equation

HRID 601659 reaction equation
[Br:1][C:2]1[CH:13]=[CH:12][C:5]2[C:6](=[O:11])[NH:7][C:8](=O)O[C:4]=2[CH:3]=1.C[NH2:15].CO>>[CH3:8][NH:7][C:6](=[O:11])[C:5]1[CH:12]=[CH:13][C:2]([Br:1])=[CH:3][C:4]=1[NH2:15]

Participants

3

Reactant 2

HCID 21331325HCID 21331325, compoundHCID 57454252Monomethylamine methanol

Product 1

HCID 23158201HCID 23158201, compound

Procedure

30 ml of 2.0 M methylamine-methanol solution was added to 6.28 mg of 7-bromo-1H-benzo[1,3]oxazine-2,4-dion, and the mixture was stirred at room temperature for 2 hours. The reaction solution was distilled outunder reduced pressure, to obtain 6.57 mg of the above compound.

Workup

  1. distillationThe reaction solution was distilled outunder reduced pressure

Sources & evidence

ORD record
ord-7e3e8c30105142ccabb45d6a3c40bb13
Source dataset
uspto-grants-2011_03
Patent number
US07902369B2

Reaction notes

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