反应详情

温度

50 °C

A mixture of 63 g of 2-methyl-4-oxatricyclo[5.2.1.02,6]-decan-3-ol, 42 g of pyridine, and 51 g of acetic anhydride was heated at 50° C. for 5 hours. The reaction mixture was concentrated. The concentrate was purified by distillation, obtaining 74 g (yield 96%) of the target compound.

1. concentrationThe reaction mixture was concentrated
2. distillationThe concentrate was purified by distillation