Sodium Hydroxide → HCID 50898814, compound

HRID 601951Notes

Reaction equation

HRID 601951 reaction equation
C([O:3][C:4]([C:6]1[NH:7][C:8]2[CH2:9][C@@H:10]3[C@H:14]([CH3:15])[C@@H:11]3[C:12]=2[CH:13]=1)=[O:5])C.[OH-].[Na+]>>[CH3:15][C@H:14]1[C@H:10]2[CH2:9][C:8]3[NH:7][C:6]([C:4]([OH:5])=[O:3])=[CH:13][C:12]=3[C@@H:11]12

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 59180173HCID 59180173, compound

Product 1

HCID 50898814HCID 50898814, compound

Procedure

The title compound was synthesized from ±(1S,1aS,5aR)-1-methyl-1a,4,5,5a-tetrahydro-1H-4-aza-cyclopropa[α]pentalene-3-carboxylic acid ethyl ester (0.12 g, 0.585 mmol) and sodium hydroxide (1.5M, 3.1 mL) according to General Procedure 7 to afford the title compound. LC-MS: MS m/z: 178 (M+1).

Sources & evidence

ORD record
ord-4e9b1c1b51344068a07766c6ca385968
Source dataset
uspto-grants-2011_03
Patent number
US07902252B2

Reaction notes

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