Phosphorodithioic acid → Phosphorodithioic acid, zinc salt (1:?)

Temperature

65 °C

To a three neck flask was added 204.3 g of the dithiophosphoric acid mixture from Example 3, lot RJT-543-244, and 27.1 g of zinc oxide. The mixture was heated to 65° C. and mixed at this temperature for four hours. The temperature was then increased to 100° C. The temperature was then gradually increased to 110° C. under vacuum while distilling off any water produced from the reaction. After mixing at 110° C. for 1 hour while under vacuum, the final product was filtered with diatomaceous earth.

1. additionmixed at this temperature for four hours
2. temperatureThe temperature was then increased to 100° C
3. temperatureThe temperature was then gradually increased to 110° C. under vacuum
4. distillationwhile distilling off any water
5. customproduced from the reaction
6. additionAfter mixing at 110° C. for 1 hour while under vacuum
7. filtrationthe final product was filtered with diatomaceous earth

ORD record

ord-655e084eea684383a72d73073ec898d5

Source dataset

uspto-grants-2011_03

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US07902403B2