Ammonium Chloride → HCID 66645954, compound

HRID 602316Notes

Reaction equation

HRID 602316 reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([C:7](=[O:21])[N:8](C)C(C)[N:10]2[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:5][CH:4]=1.[Cl-].[NH4+]>>[NH:10]([C:11]1[CH:12]=[C:3]([O:2][CH3:1])[CH:4]=[CH:5][C:6]=1[C:7]([NH2:8])=[O:21])[C:13]1[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1

Participants

3

Reactant 2

HCID 25517Ammonium ChlorideHCID 11219789HCID 11219789, compound

Product 1

HCID 66645954HCID 66645954, compound

Procedure

Following the procedure for 7-methoxy-2,3-dimethyl-1-phenyl-2,3-dihydroquinazolin-4(1H)-one (Step B), using ammonium chloride in place of methylamine hydrochloride, 2-anilino-4-methoxybenzamide was obtained.

Sources & evidence

ORD record
ord-07bb77e853364d6abdc3917e5fe966ef
Source dataset
uspto-grants-2011_03
Patent number
US07906521B2

Reaction notes

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