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HRID602355

反应详情

EQUATION

反应方程式

HRID 602355 的结构方程式

REACTANTS

反应物

2
结构：N#Cc1ccccc1Cn1c(Cl)cc(=O)[nH]c1=O
HCID11357468

2-[(6-Chloro-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)methyl]benzonitrile

C12H8ClN3O2

结构：Cn1c(=O)cc(N2CCCC(N)C2)n(Cc2ccccc2C#N)c1=O.O=C(O)c1ccccc1
HCID66697752

未命名化合物

PRODUCTS

生成物

1
结构：N#Cc1ccccc1Cn1c(N2CCC[C@@H](N)C2)cc(=O)[nH]c1=O
HCID11278798

未命名化合物

PROCEDURE

实验过程

The title compound 6 was prepared from compound 2 by the procedure used in preparation of compound 4. 1H-NMR (400 MHz, CDCl3-CD3OD 10:1): δ 7.65 (d, J=7.5 Hz, 1H), 7.58 (t, J=7.8 Hz, 1H), 7.39 (t, J=7.5 Hz, 1H), 7.27 (d, J=7.8 Hz, 1H), 5.32 (s, 1H), 5.13-5.13 (ABq, 2H, J=30.0, 15.0 Hz), 3.39 (m, 2H), 2.95 (m, 2H), 2.69 (m, 1H), 2.12 (m, 1H), 1.85 (m, 1H), 1.64 (m, 2H). MS (ES) [m+H] calc'd for C17H20N5O2, 326.2; found, 326.2.