Oxalic Acid → HCID 86624152, compound

Participants

Reaction Steps

A mixture of N-[(3S,5R)-5-(3-hydroxypropyl)pyrrolidin-3-yl]-1-isopropyl-1H-indazole-3-carboxamide (39 mg, 0.12 mmol, step 8 of Example 8) and oxalic acid (11 mg, 0.12 mmol) in dichloromethane-methanol (5 mL-1 mL) was stirred for 1 h. The mixture was concentrated to give 40 mg (81%) of the title compound as a white amorphous solid.

Provenance & Evidence