HCID 9950375, compound → HCID 9863508, compound

HRID 603278Notes

Reaction equation

HRID 603278 reaction equation
[C:1]([O:4][C:5]1[CH:6]=[C:7]([CH:24]=[CH:25][CH:26]=1)[C:8]1[C:17](=[O:18])[C:16]2[C:11](=[C:12]([CH3:23])[C:13]([O:19][C:20](=[O:22])[CH3:21])=[CH:14][CH:15]=2)[O:10][CH:9]=1)(=[O:3])[CH3:2]>CO.[Pd]>[C:1]([O:4][C:5]1[CH:6]=[C:7]([CH:24]=[CH:25][CH:26]=1)[CH:8]1[CH:17]([OH:18])[C:16]2[C:11](=[C:12]([CH3:23])[C:13]([O:19][C:20](=[O:22])[CH3:21])=[CH:14][CH:15]=2)[O:10][CH2:9]1)(=[O:3])[CH3:2]

Participants

4

Reactant 1

HCID 9950375HCID 9950375, compound

Product 1

HCID 9863508HCID 9863508, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

3′,7-Diacetoxy-8-methylisoflavan-4-ol was prepared from 3′,7-diacetoxy-8-methylisoflavone (0.25 g, 0.7 mmol) in methanol (50 ml) using palladium-on-charcoal (5%, 0.06 g) by the method described above.

Sources & evidence

ORD record
ord-fea1eb62888d46d6b9ea91caa4dfbbd5
Source dataset
uspto-grants-2011_03
Patent number
US07906660B2

Reaction notes

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