HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorophenol → N-(2',6'-dichlorophenyl)-N-chloroacetyl-4-methylaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorophenol | HCID 6899 | — |
| Reactant | 2-Chloro-N-(4-methylphenyl)acetamide | HCID 27967 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-(2',6'-dichlorophenyl)-N-chloroacetyl-4-methylaniline | HCID 57952147 | — |
Reaction Steps
Same procedure as example 6a starting from 2,6-dichlorophenol and 2-chloro-N-(4-methylphenyl)acetamide. At the end of the acetylation reaction the mixture was diluted with a small amount of toluene (0.2 part) to prevent solidification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07906677B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-af3bd9ab2c584e5988f942de2ef192e8 |
| Source note | uspto-grants-2011_03 |