HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Phenyl-o-phenylenediamine → 2-(3-Bromophenyl)-1-phenyl-1H-benzoimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Phenyl-o-phenylenediamine | HCID 68297 | — |
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Reactant | 2-(4-Bromophenyl)-1-phenyl-1H-benzo(d)imidazole | HCID 23094070 | — |
| Product | 2-(3-Bromophenyl)-1-phenyl-1H-benzoimidazole | HCID 23094065 | — |
Reaction Steps
2-(3-Bromophenyl)-1-phenyl-1H-benzo[d]imidazole (m-BPBI) was prepared as the same procedure as 2-(4-bromophenyl)-1-phenyl-1H-benzo[d]imidazole from N-phenyl-o-phenylenediamine and 4-bromobenzaldehyde. The isolated yield of the compound was 85%. It has the same spectroscopic data as that as the bona fide compound.11
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07910228B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-97ac8f320adc4c73b20b6977dc4bae6b |
| Source note | uspto-grants-2011_03 |