HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59715735, compound → HCID 59715643, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59715735 | HCID 59715735 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 59715643 | HCID 59715643 | 10.4% |
Reaction Steps
Palladium-carbon (10%, 5.0 mg) was added to a solution of the compound of Example B158 (2.0 mg) in tetrahydrofuran (2.0 ml), and the mixture was stirred at room temperature under nitrogen atmosphere (1 atm) for 1 hour. The catalyst was removed by filtration, and the filtrate was concentrated. The residue was purified by silica gel column chromatography to give the title compound (0.21 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07910712B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-82806c6464d042f599f0fa3571e20f28 |
| Source note | uspto-grants-2011_03 |