4-Bromobenzylamine → HCID 60724410, compound

HRID 605082Notes

Reaction equation

[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12].[Br:14][C:15]1[CH:22]=[CH:21][C:18]([CH2:19][NH2:20])=[CH:17][CH:16]=1>>[Br:14][C:15]1[CH:22]=[CH:21][C:18]([CH2:19][NH:20][C:6](=[O:7])[C:5]2[CH:9]=[CH:10][C:2]([Cl:1])=[C:3]([N+:11]([O-:13])=[O:12])[CH:4]=2)=[CH:17][CH:16]=1

Participants

Reactant 2

HCID 775714-Bromobenzylamine

HCID 1234774-Chloro-3-nitrobenzoyl chloride

Product 1

HCID 60724410HCID 60724410, compound

Procedure

A mixture of 4-chloro-3-nitrobenzoyl chloride was reacted with 4-Bromo-benzylamine to produce N-(4-Bromo-benzyl)-4-chloro-3-nitro-benzamide according to the procedure of Example 10A, which was treated sequentially using the procedures from Examples 22A and 22B to provide the title product.

Sources & evidence

ORD record: ord-d1ea27d6a1774a32b41a40587f81faae
Source dataset: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07910595B2

Reaction notes

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