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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 605096Generated: October 31, 2026

Toluene → HCID 86615545, compound

https://huagongshe.com/reaction/605096

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTolueneHCID 1140—
ReactantThionyl ChlorideHCID 24386—
ReactantHCID 67041002HCID 67041002—
ProductHCID 86615545HCID 86615545—

Reaction Steps

A solution of the product from Example 43C (224 mg, 0.443 mmol) in thionyl chloride (2 mL) was refluxed for 1 hour. The mixture was cooled to room temperature, toluene (5 mL) was added and the mixture concentrated under vacuum to provide the title product as a solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07910595B2
Source datasetuspto-grants-2011_03
ORD IDord-6bfca08f7c7d49d39a7948b3c4b09c97
Source noteuspto-grants-2011_03