3-Bromoaniline → N-(3-bromophenyl)-4-chloro-3-nitrobenzamide

HRID 605113Notes

Reaction equation

HRID 605113 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12].[Br:14][C:15]1[CH:16]=[C:17]([NH2:21])[CH:18]=[CH:19][CH:20]=1>>[Br:14][C:15]1[CH:16]=[C:17]([NH:21][C:6](=[O:7])[C:5]2[CH:9]=[CH:10][C:2]([Cl:1])=[C:3]([N+:11]([O-:13])=[O:12])[CH:4]=2)[CH:18]=[CH:19][CH:20]=1

Participants

3

Reactant 2

HCID 115623-BromoanilineHCID 1234774-Chloro-3-nitrobenzoyl chloride

Product 1

HCID 1368133N-(3-bromophenyl)-4-chloro-3-nitrobenzamide

Procedure

A mixture of 4-chloro-3-nitrobenzoyl chloride was reacted with 3-Bromo-phenylamine to produce N-(3-Bromo-phenyl)-4-chloro-3-nitro-benzamide according to the procedure of Example 10A, which was treated sequentially using the procedures from Examples 13A, 13B and 13C to provide the title product.

Sources & evidence

ORD record
ord-7199aa0803f1432d88b9269241ddffef
Source dataset
uspto-grants-2011_03
Patent number
US07910595B2

Reaction notes

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