Aniline → Benzamide, 4-chloro-3-nitro-N-phenyl-

HRID 605121Notes

Reaction equation

[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12].[C:14]1([NH2:20])[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1>>[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH:20][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12]

Participants

Reactant 2

HCID 6115Aniline

HCID 1234774-Chloro-3-nitrobenzoyl chloride

Product 1

HCID 96073Benzamide, 4-chloro-3-nitro-N-phenyl-

Procedure

A mixture of 4-chloro-3-nitrobenzoyl chloride was reacted with Phenylamine to produce 4-Chloro-3-nitro-N-phenyl-benzamide according to the procedure of Example 10A, which was treated sequentially using the procedures from Examples 22A and 22B to provide the title product.

Sources & evidence

ORD record: ord-900fe1bba1ee40f6b715ac2b42fd16d1
Source dataset: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07910595B2

Reaction notes

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