4-Fluoro-m-toluidine → HCID 62811803, compound

HRID 605129Notes

Reaction equation

HRID 605129 reaction equation
[F:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12].[F:14][C:15]1[CH:20]=[CH:19][C:18]([NH2:21])=[CH:17][C:16]=1[CH3:22]>>[F:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH:21][C:18]2[CH:19]=[CH:20][C:15]([F:14])=[C:16]([CH3:22])[CH:17]=2)=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12]

Participants

3

Reactant 2

HCID 679814-Fluoro-m-toluidineHCID 27833474-Fluoro-3-nitrobenzoyl chloride

Product 1

HCID 62811803HCID 62811803, compound

Procedure

A mixture of the product from Example 86A was reacted with 4-Fluoro-3-methyl-phenylamine to produce 4-Fluoro-N-(4-fluoro-3-methyl-phenyl)-3-nitro-benzamide according to the procedure of Example 86B, which was treated sequentially using the procedures from Examples 86C and 395D to provide the title product.

Sources & evidence

ORD record
ord-b3542f55357e4e7cbc6f9e72979c78a0
Source dataset
uspto-grants-2011_03
Patent number
US07910595B2

Reaction notes

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