4-Bromophenylhydrazine → HCID 67040603, compound

HRID 605156Notes

Reaction equation

[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12].[Br:14][C:15]1[CH:20]=[CH:19][C:18]([NH:21][NH2:22])=[CH:17][CH:16]=1>>[Br:14][C:15]1[CH:20]=[CH:19][C:18]([NH:21][NH:22][C:6](=[O:7])[C:5]2[CH:9]=[CH:10][C:2]([Cl:1])=[C:3]([N+:11]([O-:13])=[O:12])[CH:4]=2)=[CH:17][CH:16]=1

Participants

Reactant 2

HCID 121584-Bromophenylhydrazine

HCID 1234774-Chloro-3-nitrobenzoyl chloride

Product 1

HCID 67040603HCID 67040603, compound

Procedure

A mixture of 4-chloro-3-nitrobenzoyl chloride was reacted with (4-Bromo-phenyl)-hydrazine to produce 4-Chloro-3-nitro-benzoic acid N′-(4-bromo-phenyl)-hydrazide according to the procedure of Example 10A, which was treated sequentially using the procedures from Examples 100A, 100B and 100C to provide the title product.

Sources & evidence

ORD record: ord-c6281856a6cd4b93b349c1deec5bb93d
Source dataset: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07910595B2

Reaction notes

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