HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86615557, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 67040552 | HCID 67040552 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86615557 | HCID 86615557 | — |
Reaction Steps
The product from Example 162a (2.0 g, 42.9 mmol) in thionyl chloride (10 mL) containing 1 drop of dimethylformamide and was heated to reflux for 3 hours. Cooled and concentrated under vacuum and dried under high vacuum overnight. The title compound was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07910595B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-6ba33d48e02f47c88cde4080427ce11e |
| Source note | uspto-grants-2011_03 |