Ammonium Chloride → HCID 67040258, compound

Participants

Reaction Steps

The product of Example 166A (340 mg, 0.6197 mmol) was reduced with Fe and NH4Cl following the procedure in Example 9E to yield the title compound (231 mg, 72% yield) as a white solid. 1H NMR (300 MHz, DMSO-D6) δ ppm: 4.94 (s, 2 H) 5.59 (s, 2 H) 7.14-7.35 (m, 4 H) 7.42 (s, 1 H) 7.50 (d, J=8.46 Hz, 2 H) 9.22 (s, 1 H) 10.26 (s, 1 H); MS (ESI) m/z 520 (M+H)+.

Provenance & Evidence