Potassium Hydroxide → HCID 67040570, compound

Participants

Reaction Conditions

Reaction Steps

The product from Example 172b (215 mg, 0.655 mmol) was dissolved in DMSO (30 ml) to which KOH (75 mg, 1.31 mmol) and (4-Hydroxy-phenyl)-carbamic acid tert-butyl ester (137 mg, 0.655 mmol) were added. The reaction mixture was then heated to 80° C. for 2 h reaction mixture was then cooled to room temperature and diluted with water and the title compound collected by filtration (240 mg, 78%).

Provenance & Evidence