4-Chloro-2,6-dimethylaniline → HCID 67041118, compound

HRID 605210Notes

Reaction equation

HRID 605210 reaction equation
[Cl:1][C:2]([Cl:28])([Cl:27])[CH2:3][O:4][C:5](=[O:26])[NH:6][C:7]1[CH:12]=[CH:11][C:10]([S:13][C:14]2[CH:19]=[CH:18][C:17]([C:20](Cl)=[O:21])=[CH:16][C:15]=2[N+:23]([O-:25])=[O:24])=[CH:9][CH:8]=1.[Cl:29][C:30]1[CH:35]=[C:34]([CH3:36])[C:33]([NH2:37])=[C:32]([CH3:38])[CH:31]=1>C1(C)C=CC=CC=1>[Cl:1][C:2]([Cl:28])([Cl:27])[CH2:3][O:4][C:5](=[O:26])[NH:6][C:7]1[CH:12]=[CH:11][C:10]([S:13][C:14]2[CH:19]=[CH:18][C:17]([C:20](=[O:21])[NH:37][C:33]3[C:34]([CH3:36])=[CH:35][C:30]([Cl:29])=[CH:31][C:32]=3[CH3:38])=[CH:16][C:15]=2[N+:23]([O-:25])=[O:24])=[CH:9][CH:8]=1

Participants

4

Reactant 2

HCID 50733624-Chloro-2,6-dimethylanilineHCID 86615557HCID 86615557, compound

Product 1

HCID 67041118HCID 67041118, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The product of Example 162b (300 mg, 0.6197 mmol) and 4-Chloro-2,6-dimethyl-phenylamine (119 mg, 0.6197 mmol) were combined in toluene (10 mL) and reacted as in Example 162c to give the title compound that was used without further manipulation.

Workup

  1. customreacted as in Example 162c

Sources & evidence

ORD record
ord-ef83e27515d543b0a8c69a291769f1be
Source dataset
uspto-grants-2011_03
Patent number
US07910595B2

Reaction notes

Loading…